3-(Dimethylamino)propyl chloride hydrochloride → HCID 10384242, compound

HRID 1374518Notes

Reaction equation

HRID 1374518 reaction equation
Cl.CN(C)CCCCl.[CH3:9][N:10]([CH3:42])[CH2:11][CH2:12][CH2:13][O:14][CH2:15][C:16]1[N:25](COCC[Si](C)(C)C)[C:24]2[C:23]3[CH:34]=[CH:35][CH:36]=[CH:37][C:22]=3[S:21][C:20]3[CH:38]=[CH:39][CH:40]=[CH:41][C:19]=3[C:18]=2[N:17]=1>>[CH3:42][N:10]([CH3:9])[CH2:11][CH2:12][CH2:13][O:14][CH2:15][C:16]1[NH:17][C:18]2[C:19]3[CH:41]=[CH:40][CH:39]=[CH:38][C:20]=3[S:21][C:22]3[CH:37]=[CH:36][CH:35]=[CH:34][C:23]=3[C:24]=2[N:25]=1

Participants

3

Reactant 2

HCID 943083-(Dimethylamino)propyl chloride hydrochlorideHCID 10097321HCID 10097321, compound

Product 1

HCID 10384242HCID 10384242, compound

Procedure

By a reaction of alcohol 31 (0.58 mmole) and 3-dimethylaminopropylchloride-hydrochloride (8.1 mmole), dimethyl-{3-[1-(2-trimethylsilyl-ethoxymethyl)-1H-8-thia-1,3-diaza-dibenzo[e,h]azulene-2-ylmethoxy]-propyl}-amine in the form of an oily product was obtained;

Workup

  1. customwas obtained

Sources & evidence

ORD record
ord-c31bd1e9e9134fcc8cf5a7cfb4ac368c
Source dataset
uspto-grants-2007_01
Patent number
US07166583B2

Reaction notes

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