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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1374528Generated: October 30, 2026

Methanol → 2,5,8,11,14,17,20,23,26,29-Decaoxahentriacontan-31-ol

https://huagongshe.com/reaction/1374528

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantTriethylene GlycolHCID 8172—
Reactantm-PEG7-MsHCID 21930814—
SolventChloroformHCID 6212—
Product2,5,8,11,14,17,20,23,26,29-Decaoxahentriacontan-31-olHCID 14550547—

Reaction Steps

Monodispersed compound 32 was prepared from compound 31 and monodispersed triethylene glycol using the procedure described herein. Oil; Rf 0.41 (methanol: chloroform=6:10); MS m/z calc'd for C21H44O11 472.29 (M++1), found 472.29.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07166571B2
Source datasetuspto-grants-2007_01
ORD IDord-16c6d3107b024b3393eecbed4a067055
Source noteuspto-grants-2007_01