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HRID1374557

反应详情

EQUATION

反应方程式

HRID 1374557 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CN1C(=O)[C@@H](NC(=O)OC(C)(C)C)CNc2ccccc21
HCID57617767

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)N1C[C@H](NC(=O)OC(C)(C)C)C(=O)N(C)c2ccccc21
HCID69043281

未命名化合物

PROCEDURE

实验过程

In an analogous manner to that described in Example 56 b), the acylation of (S)-(1-methyl-2-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-carbamic acid tert-butyl ester [Example 56 a)] with acetic acid anhydride yielded the title compound as a white solid; MS: m/e=334 (M+H)+.