HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → HCID 54111983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | Benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate | HCID 151348 | — |
| Reactant | L-tert-Leucine | HCID 164608 | — |
| Reactant | HCID 131723874 | HCID 131723874 | — |
| Product | HCID 54111983 | HCID 54111983 | — |
| Product | HCID 131723873 | HCID 131723873 | — |
Reaction Steps
N-(Toluene-4-sulfonyl)-L-tert-butylglycine was prepared from L-tert-butylglycine using the procedure described in Method 1. The title compound was prepared by coupling in DMF N-(toluene-4-sulfonyl)-L-tert-butylglycine with an L-phenylalanine ester in the presence of BOP and NMM. Conventional deesterification provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166580B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-6866740b7fe34eaeba9c68e1c6363356 |
| Source note | uspto-grants-2007_01 |