HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5,6-Dichloro-3-pyridyloxy)butyric acid → 2-(5,6-dichloro-3-pyridyloxy)-N-(1-tert-butyldimethylsilyloxy-4-methylpent-2-yn-4-yl)butyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5,6-Dichloro-3-pyridyloxy)butyric acid | HCID 21078365 | — |
| Reactant | 4-Amino-1-tert-butyldimethylsilyloxy-4-methylpent-2-yne | HCID 21923134 | — |
| Product | 2-(5,6-dichloro-3-pyridyloxy)-N-(1-tert-butyldimethylsilyloxy-4-methylpent-2-yn-4-yl)butyramide | HCID 87788031 | — |
Reaction Steps
In a similar procedure to that described in Example 11 Stage 3, the product from Step 2 was reacted with 4-amino-1-tert-butyldimethylsilyloxy-4-methylpent-2-yne to give 2-(5,6-dichloro-3-pyridyloxy)-N-(1-tert-butyldimethylsilyloxy-4methylpent-2-yn-4-yl)butyramide as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166621B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-04e3547de96f495dbd2db5e1f2e78565 |
| Source note | uspto-grants-2007_01 |