HCID 21078429, compound → HCID 21078396, compound

HRID 1374913Notes

Reaction equation

HRID 1374913 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([O:9][CH:10]([CH2:14][CH3:15])[C:11]([OH:13])=O)[CH:6]=[N:7][CH:8]=1)#[N:2].Cl.[NH2:17][C:18]([CH3:23])([CH3:22])[C:19]#[C:20][CH3:21]>>[C:1]([C:3]1[CH:4]=[C:5]([O:9][CH:10]([CH2:14][CH3:15])[C:11]([NH:17][C:18]([CH3:23])([CH3:22])[C:19]#[C:20][CH3:21])=[O:13])[CH:6]=[N:7][CH:8]=1)#[N:2]

Participants

3

Reactant 2

HCID 21078429HCID 21078429, compoundHCID 219231292-Methylpent-3-yn-2-amine hydrochloride

Product 1

HCID 21078396HCID 21078396, compound

Procedure

The product from Step 2 was condensed with 4-amino-4-methylpent-2-yne hydrochloride in a similar procedure to that described in Example 1 Stage 3 to give the required product as a colourless solid, m.p. 112–113° C.

Sources & evidence

ORD record
ord-3ceceac3544f49c6aa34f8715d5eef4a
Source dataset
uspto-grants-2007_01
Patent number
US07166621B2

Reaction notes

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