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HRID1375057

反应详情

EQUATION

反应方程式

HRID 1375057 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)NS(=O)(=O)c1sc(Cl)cc1N
HCID10967526

3-Amino-N-tert-butyl-5-chlorothiophene-2-sulfonamide

C8H13ClN2O2S2

PRODUCTS

生成物

1
结构：Nc1cc(Cl)sc1S(N)(=O)=O
HCID10955934

未命名化合物

收率 100.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

A solution of 3a (250 mg, 0.93 mmol) in concentrated HCl solution (10 mL) was heated at 55° C. for 2h. Removal of all solvents then afforded 3b (198 mg) as a yellow solid.

WORKUP

后处理

  1. customRemoval of all solvents