Chlorobenzene → HCID 69263909, compound

HRID 1375060Notes

Reaction equation

HRID 1375060 reaction equation
[NH2:1][C:2]1[CH:6]=[C:5](Cl)[S:4][C:3]=1[S:8]([NH2:11])(=[O:10])=[O:9].[Cl:12][C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1>>[NH2:1][C:2]1[CH:6]=[C:5]([C:17]2[CH:16]=[CH:15][CH:14]=[C:13]([Cl:12])[CH:18]=2)[S:4][C:3]=1[S:8]([NH2:11])(=[O:10])=[O:9]

Participants

3

Reactant 2

HCID 7964ChlorobenzeneHCID 109559343-Amino-5-chlorothiophene-2-sulfonamide

Product 1

HCID 69263909HCID 69263909, compound

Procedure

The title compound was prepared from 3-chlorobenzene boronic acide and 3b by following the procedure in example 3c. This compound is a white solid: MS (ES) 289 (M+H)+; 1H NMR (400 MHz, CD3OD) δ7.62 (s 1 H), 7.53 (m, 1 H), 7.40 (m, 2 H), 6.92 (s, 1 H).

Sources & evidence

ORD record
ord-22c56c4137a24fe1a850595116153214
Source dataset
uspto-grants-2007_01
Patent number
US07166639B2

Reaction notes

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