Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Methylquinoline | HCID 10285 | — |
| Reactant | 6-Bromohexanoic acid | HCID 20210 | — |
| Product | HCID 11772090 | HCID 11772090 | 88.9% |
Reaction Steps
See FIG. 3B. A mixture of lepidine (5 g) and 6-bromohexanoic acid (10 g) was heated to 130° C. for 6 h. The solid was washed with acetone and filtered to provide an off-white solid (10.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07166715B2 |
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| Source dataset | uspto-grants-2007_01 |
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| ORD ID | ord-0b0fa9859cdd478281f8f0818f2e8cfc |
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| Source note | uspto-grants-2007_01 |
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