HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 3-(sec-butylcarbamoyl)acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 3-(Sec-butylcarbamoyl)acrylic acid | HCID 244595 | — |
| Product | Methyl 3-(sec-butylcarbamoyl)acrylate | HCID 54128810 | — |
Reaction Steps
To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166748B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-5d1699450511463e996bfab6b995d881 |
| Source note | uspto-grants-2007_01 |