HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 11608505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 11615748 | HCID 11615748 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 11608505 | HCID 11608505 | — |
Reaction Steps
lin 300 ml methanol 8.4 g (33.7 mmol) of trans-2-methoxy-4-(6-nitro-cyclohex-3-enyl)-phenol are solved. To this solution 500 mg of 10% Pd/C are added. The mixture is hydrogenated at room temperature for 6 hours. The mixture was then filtered through Filter Cel and evaporation of the filtrate in vacuum, yielding trans-2 methoxy-4-(2-nitro-cyclohexyl)-phenol as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166746B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-7f2705ea44f94342a2dc7d26c6485ed3 |
| Source note | uspto-grants-2007_01 |