HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[[4-[2-(Diethylamino)ethoxy]phenyl]amino]-4-(methylamino)-5-nitropyrimidine → 5-Amino-2-[[4-[2-(diethylamino)ethoxy]phenyl]amino]-4-(methylamino)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[[4-[2-(Diethylamino)ethoxy]phenyl]amino]-4-(methylamino)-5-nitropyrimidine | HCID 58786795 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5-Amino-2-[[4-[2-(diethylamino)ethoxy]phenyl]amino]-4-(methylamino)pyrimidine | HCID 58786778 | — |
Reaction Steps
Hydrogenation of 2-[[4-[2-(diethylamino)ethoxy]phenyl]amino]-4-(methylamino)-5-nitropyrimidine (from Example 2(2) above) over Pd/C gave the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169778B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-f9b989ad72444d1c9145810d98fc5461 |
| Source note | uspto-grants-2007_01 |