HCID 52949450, compound → HCID 58786789, compound

HRID 1375402Notes

Reaction equation

HRID 1375402 reaction equation
[CH:1]1([NH:6][C:7]2[C:12]([N+:13]([O-])=O)=[CH:11][N:10]=[C:9]([NH:16][C:17]3[CH:22]=[CH:21][N:20]=[CH:19][CH:18]=3)[N:8]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1>[Pd]>[NH2:13][C:12]1[C:7]([NH:6][CH:1]2[CH2:5][CH2:4][CH2:3][CH2:2]2)=[N:8][C:9]([NH:16][C:17]2[CH:18]=[CH:19][N:20]=[CH:21][CH:22]=2)=[N:10][CH:11]=1

Participants

3

Reactant 1

HCID 52949450HCID 52949450, compound

Product 1

HCID 58786789HCID 58786789, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Hydrogenation of 4-(cyclopentylamino)-2-[(pyridin4-yl)amino]-5-nitropyrimidine (from Example 2(6) above) over Pd/C gave the title compound as a solid.

Sources & evidence

ORD record
ord-9321caba11844109b991654f9112b750
Source dataset
uspto-grants-2007_01
Patent number
US07169778B2

Reaction notes

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