HCID 58786791, compound → HCID 58786800, compound

HRID 1375403Notes

Reaction equation

HRID 1375403 reaction equation
[CH2:1]([N:3]([CH2:26][CH3:27])[CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH:13][C:14]2[N:19]=[C:18]([NH:20][CH2:21][CH3:22])[C:17]([N+:23]([O-])=O)=[CH:16][N:15]=2)=[CH:9][CH:8]=1)[CH3:2]>[Pd]>[NH2:23][C:17]1[C:18]([NH:20][CH2:21][CH3:22])=[N:19][C:14]([NH:13][C:10]2[CH:9]=[CH:8][C:7]([O:6][CH2:5][CH2:4][N:3]([CH2:26][CH3:27])[CH2:1][CH3:2])=[CH:12][CH:11]=2)=[N:15][CH:16]=1

Participants

3

Reactant 1

HCID 58786791HCID 58786791, compound

Product 1

HCID 58786800HCID 58786800, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Hydrogenation of 2-[[4-[2-(diethylamino)ethoxy]phenyl]amino]-4-(ethylamino)-5-nitropyrimidine (from Example 2(7) above) over Pd/C gave the title compound as an oil.

Sources & evidence

ORD record
ord-623f4a28483e4ccbb56ec9d57c1f35aa
Source dataset
uspto-grants-2007_01
Patent number
US07169778B2

Reaction notes

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