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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1375520Generated: October 31, 2026

Potassium Carbonate → HCID 21897138, compound

https://huagongshe.com/reaction/1375520

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant6-chloro-N-(3-chloro-4-methoxyphenyl)-N'-cycloheptyl-[1,3,5]triazine-2,4-diamineHCID 21897021—
SolventMethanolHCID 887—
ProductHCID 21897138HCID 21897138—

Reaction Steps

To 6-chloro-N-(3-chloro-4-methoxyphenyl)-N′-cycloheptyl-[1,3,5] triazine-2,4-diamine (5 g) dissolved in methanol was added K2CO3 (3.2 g) and refluxed for about 6–8 h. TLC was monitored. After the completion of the reaction, the reaction mass was filtered through vacuum and the filtrate was evaporated to yield the title compound. (Wt. 4.7 g Y: 95%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07169785B2
Source datasetuspto-grants-2007_01
ORD IDord-561ac9a0f262483d9f3b867d68ee6d67
Source noteuspto-grants-2007_01