HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1375541Generated: October 31, 2026
4-Fluorobenzylamine → HCID 54711989, compound
https://huagongshe.com/reaction/1375541
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Fluorobenzylamine | HCID 67326 | — |
| Reactant | HCID 17961872 | HCID 17961872 | — |
| Reactant | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54711989 | HCID 54711989 | — |
Reaction Steps
The crude product of Step 2 was dissolved in MeOH and 4-fluorobenzylamine (3.5 eq.) added. The solution was stirred at 60° C. over night. The title product was obtained by preparative RP-HPLC (C18, gradient of CH3CN/H2O+0.01% TFA).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07169780B2 |
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| Source dataset | uspto-grants-2007_01 |
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| ORD ID | ord-449d99931b5440e7abd040667a1cd715 |
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| Source note | uspto-grants-2007_01 |
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