HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59442734, compound → 3-Amino-N-methyl-5-(trifluoromethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59442734 | HCID 59442734 | — |
| Reactant | HCID 59631038 | HCID 59631038 | — |
| Product | 3-Amino-N-methyl-5-(trifluoromethyl)benzamide | HCID 57431453 | — |
Reaction Steps
Utilising the procedure described in Example 86e, but employing α,α,α-trifluoro-N-methyl-5-nitro-m-toluamide (Dean E. Welch, J. Med. Chem. (1969),12, 299–303) in lieu of 3-(4-morpholinyl)-5-nitro-N-(methyl)-benzamide, afforded the title compound as a beige crystalline solid, m.p. 113–115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169791B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-0016656ef7e348cdb35ee376bf8f9d2f |
| Source note | uspto-grants-2007_01 |