HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-isocyanato-2-methoxy- → HCID 69352904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-isocyanato-2-methoxy- | HCID 69695 | — |
| Reactant | HCID 22667151 | HCID 22667151 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 69352904 | HCID 69352904 | 95% |
Reaction Steps
4-[(6,7-Dimethoxy-4-quinazolinyl)oxy]-2-methylaniline (50 mg) was dissolved in chloroform (3 ml), and 2-methoxyphenyl isocyanate (26 μl) was then added to the solution. The mixture was heated under reflux overnight. The precipitated crystal was collected by filtration and was washed to give 70 mg (yield 95%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169789B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-0a49cb86bf974f22be31fb47f6221c39 |
| Source note | uspto-grants-2007_01 |