HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → HCID 58788422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | N-(2-Cyano-3-fluorophenyl)-2,2,2-trifluoroacetamide | HCID 54264547 | — |
| Product | HCID 58788422 | HCID 58788422 | — |
Reaction Steps
Follow the procedure of Example 5, but start with 3-fluoro-N-(2-cyano-phenyl)-2,2,2-trifluoroacetamide (synthesis described in J. Fluorine Chem. 1981, 18, (2), 185–95) and tert-butyl bromoacetate to obtain the title compound: MS 251(M+H), TLC (silica gel, dichloromethane/methanol, 7:1) Rf=0.38.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169925B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-20d84f22d66345199d763b82524f56db |
| Source note | uspto-grants-2007_01 |