HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 22916502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 22916503 | HCID 22916503 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22916502 | HCID 22916502 | 36.3% |
Reaction Steps
1.5 g (0.0061 mol) of 2'-nitro-3'-chloro-2-(methylthio)acetophenone are prepared by addition at 0° C. of 1.3 g (0.018 mol) of sodium methanethiolate in solution in 10 ml of methanol to 4.7 g (0.0168 mol) of 2'-nitro-3'-chloro-2-bromoacetophenone obtained above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663119 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-f4ea00ceebf544eba32d3b5e14f9a881 |
| Source note | uspto-grants-1997_09 |