HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbonate Ion → 1-(8-Bromooctyl)-4,5-diphenyltriazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbonate Ion | HCID 19660 | — |
| Reactant | 1,8-Dibromooctane | HCID 78310 | — |
| Reactant | HCID 178420171 | HCID 178420171 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 1-(8-Bromooctyl)-4,5-diphenyltriazole | HCID 22916394 | — |
Reaction Steps
4,5-Diphenyl-1,2,3-triazole was treated with 1,8-dibromooctane and potassinm carbonate in butanone to give after chromatographic work up the title compound, m.p. 90°-91° C, Found: C, 64.0; H, 6.5; N, 10.1; Br, 19.8%; C22H26BrN3 requires: C, 64.1; H, 6.4; N, 10.2; Br, 19.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663053 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-02f1d1d8606d4b4cac4393c7c8eacb94 |
| Source note | uspto-grants-1997_09 |