HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22916458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4,5-Triphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 628544 | — |
| Reactant | HCID 22916460 | HCID 22916460 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 22916458 | HCID 22916458 | — |
Reaction Steps
1,4,5-Triphenylimidazol-2-one was treated with ethyl 9-bromo-undecanoate and potassium carbonate in butanone, followed by sodium hydroxide in ethanol and water, to give after work-up the title compound, m.p. 83°-84° C. Found: C, 77.5; H, 7.3; N, 5.4%; C32H36N2O3 requires: C, 77.4; H, 7.3; N, 5.6%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663053 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-879ae00bb59347be926652eb4e7977d6 |
| Source note | uspto-grants-1997_09 |