HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 21840485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 21840487 | HCID 21840487 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21840485 | HCID 21840485 | — |
Reaction Steps
To a stirred solution of 0.78 g of 5-isothiocyanato-4-methyl-1,3-benzodioxole in 50 mL of toluene at 25° C. is added 0.80 mL of ethylenediamine. After five minutes, the mixture is concentrated under reduced pressure to yield 1.0 g of 5-[N'-(2-aminoethyl)thioureido]-4-methyl-1,3-benzodioxole as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663189 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-bd2f212bc1a543f1b185cce9605a2dd1 |
| Source note | uspto-grants-1997_09 |