HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacryloyl chloride → HCID 86751205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Hydroxyethyloxamic acid | HCID 165301 | — |
| Reactant | Methacryloyl isocyanate | HCID 10942374 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 86751205 | HCID 86751205 | — |
Reaction Steps
In example 1, when the reaction of a triethylamine salt of 2-hydroxyethyloxamic acid with methacrylic acid chloride was performed, 5.5 g (0.05 moles) of methacryloylisocyanate were used instead of methacrylic acid chloride with no use of TEA and the reaction was carried out at room temperature. Except the forementioned, the same procedure as for example 1 was carried out to get methacryloylcarbamoyloxyethyloxamic acid of the following structure. ##STR18##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663262 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-ce963b7ddc1f43c892e13ca21dba7d89 |
| Source note | uspto-grants-1997_09 |