HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butyl hydrogen N-((phenylmethoxy)carbonyl)-L-aspartate → Z-Asp(OtBu)-Val-OtBu
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butyl hydrogen N-((phenylmethoxy)carbonyl)-L-aspartate | HCID 111082 | — |
| Reactant | tert-Butyl L-valinate | HCID 114626 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | Z-Asp(OtBu)-Val-OtBu | HCID 70050186 | 93% |
Reaction Steps
By condensing Z-Asp(OtBu)-OH and H-Val-OtBu there is obtained Z-Asp(OtBu)-Val-OtBu, m.p. 75° C. (n-hexane), yield: 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663297 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-9c1a31d54e9841e09e768750a489ded0 |
| Source note | uspto-grants-1997_09 |