Chloranil → HCID 22918215, compound

HRID 1376722Notes

Reaction equation

HRID 1376722 reaction equation
[CH:1]1([N:4]2[C:13]3[C:8](=[CH:9][C:10]([F:15])=[C:11]([F:14])[CH:12]=3)[C:7](=[O:16])[CH2:6][CH2:5]2)[CH2:3][CH2:2]1.C1(Cl)C(=O)C(Cl)=C(Cl)C(=O)C=1Cl>>[CH:1]1([N:4]2[C:13]3[C:8](=[CH:9][C:10]([F:15])=[C:11]([F:14])[CH:12]=3)[C:7](=[O:16])[CH:6]=[CH:5]2)[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 8371ChloranilHCID 54256453HCID 54256453, compound

Product 1

HCID 22918215HCID 22918215, compoundYield 87%

Procedure

1-Cyclopropyl-6,7-difluoro-1,2,3,4-tetrahydro-4-oxoquinoline(10 g) and p-chloranil (22 g) were reacted in the same method as described in Preparation 1-B to give the white above-indicated compound(8.6 g).

Sources & evidence

ORD record
ord-5c415bd2c0b148fcaec719a13af0bf78
Source dataset
uspto-grants-1997_09
Patent number
US05663331

Reaction notes

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