Chloranil → HCID 22918339, compound

HRID 1376725Notes

Reaction equation

HRID 1376725 reaction equation
[CH2:1]([N:4]1[C:13]2[C:8](=[CH:9][C:10]([F:15])=[C:11]([F:14])[CH:12]=2)[C:7](=[O:16])[CH2:6][CH2:5]1)[CH:2]=[CH2:3].C1(Cl)C(=O)C(Cl)=C(Cl)C(=O)C=1Cl>>[CH2:1]([N:4]1[C:13]2[C:8](=[CH:9][C:10]([F:15])=[C:11]([F:14])[CH:12]=2)[C:7](=[O:16])[CH:6]=[CH:5]1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 8371ChloranilHCID 22918243HCID 22918243, compound

Product 1

HCID 22918339HCID 22918339, compoundYield 93.3%

Procedure

1-Allyl-6,7-difluoro-1,2,3,4-tetrahydro-4-oxoquinoline(13.3 g) and p-chloranil (29.3 g) were reacted in the same method as described in Preparation 1-B to give the white above-indicated compound(12.3 g).

Sources & evidence

ORD record
ord-c52dc73d36a4462390fad2d8c014e79c
Source dataset
uspto-grants-1997_09
Patent number
US05663331

Reaction notes

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