HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → 2-Propanone, 1-(3,4-dimethoxyphenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1,2-Dimethoxy-4-(2-nitroprop-1-enyl)benzene | HCID 95474 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Propanone, 1-(3,4-dimethoxyphenyl)- | HCID 69896 | — |
Reaction Steps
(3,4-Dimethoxyphenyl)-2-nitropropene (11) (200 g, 0.90 mol), palladium 10%/charcoal (10.0 g, either fresh or recycled), methanol (750 ml), water (220 ml) and sulfuric acid (96%, 28 ml) are charged to a steel autoclave thermostatted at 15° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663360 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-777fa9cfd86b4adfb9de1e09dcd227eb |
| Source note | uspto-grants-1997_09 |