HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoxazole → HCID 67725678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoxazole | HCID 7225 | — |
| Reactant | 1-Iodooctane | HCID 12380 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67725678 | HCID 67725678 | 73.2% |
Reaction Steps
A stirred solution of 2-methylbenzoxazole (10.0 g, 75 mmol) and n-octyl iodide (18.0 g, 75 mmol) was heated at reflux for 18 h. After cooling, the yellow-brown solid was slurried in ether, filtered and washed with ether. The resulting solid was air dried to give (20.5 g, 73%) of 3-n-octyl-2-methylbenzoxazolium iodide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05665328 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-08a2092f2b97473496cf1a6ba79b6f07 |
| Source note | uspto-grants-1997_09 |