HCID 22914913, compound → HCID 22914921, compound

Participants

Reaction Steps

500 mg (0.77 mmole) of the compound obtained in step 1 was dissolved in 8 ml of methylene chloride and to the resulting solution was added 73 mg (7.74 mmole) of manganese dioxide. The mixture was stirred for 5 hours at room temperature and the resultant was removed from the solvent and purified with silica gel column chromatography to obtain 346 mg of the title compound (yield 70%).

Provenance & Evidence