HCID 22915156, compound → HCID 54000870, compound

HRID 1377563Notes

Reaction equation

HRID 1377563 reaction equation
[N:1]([C:4]([C:11]1[S:15][C:14]([CH3:16])=[N:13][C:12]=1[CH3:17])([C:6]1[S:7][CH:8]=[CH:9][N:10]=1)[CH3:5])=[N+]=[N-]>C(O)C.[Pd]>[CH3:16][C:14]1[S:15][C:11]([C:4]([NH2:1])([C:6]2[S:7][CH:8]=[CH:9][N:10]=2)[CH3:5])=[C:12]([CH3:17])[N:13]=1

Participants

4

Reactant 1

HCID 22915156HCID 22915156, compound

Product 1

HCID 54000870HCID 54000870, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

The product from Example 19 in ethanol was hydrogenated in the presence of 10% palladium-on-charcoal to give the title compound.

Sources & evidence

ORD record
ord-6639d4d5d5b94dc1b64aa6a8b0bffd43
Source dataset
uspto-grants-1997_09
Patent number
US05665747

Reaction notes

Loading…