HCID 54047759, compound → HCID 19909636, compound

HRID 1377566Notes

Reaction equation

[C:1]([N+:4]1([O-])[CH2:9][CH2:8][C:7](=[C:10]2[C:16]3=[N:17][CH:18]=[C:19](C)[CH:20]=[C:15]3[CH2:14][CH2:13][C:12]3[CH:22]=[C:23]([Cl:26])[CH:24]=[CH:25][C:11]2=3)[CH2:6][CH2:5]1)(=[O:3])[CH3:2].O1CC[CH2:30][CH:29]1[C:33]([N:35]1CCC(=C2C3=NC=CC=C3CCC3C=C(Cl)C=CC2=3)C[CH2:36]1)=O>>[N:35]1[CH:33]=[CH:29][CH:30]=[C:2]([C:1]([N:4]2[CH2:5][CH2:6][C:7](=[C:10]3[C:16]4=[N:17][CH:18]=[CH:19][CH:20]=[C:15]4[CH2:14][CH2:13][C:12]4[CH:22]=[C:23]([Cl:26])[CH:24]=[CH:25][C:11]3=4)[CH2:8][CH2:9]2)=[O:3])[CH:36]=1

Participants

Reactant 2

HCID 54047759HCID 54047759, compound

HCID 57030266HCID 57030266, compound

Product 1

HCID 19909636HCID 19909636, compound

Procedure

1-acetyl-4-(8-chloro-5,6-dihydro-3-methyl-11 H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-ylidene)piperidine N-oxide, i.e., ##STR7## 1-acetyl-4-(3,8-dichloro-5,6-dihydro-11 H-benzo[5,6]cyclohepta-[1,2-b]pyridin-11-ylidine)piperidine N-oxide, i.e., ##STR8## 1-(2-tetrahydrofuroyl)-4-(8-chloro-5,6-dihydro-11 H-benzo[5,6]cyclohepta-[1,2-b]pyridin-11-ylidene)piperidine;

Sources & evidence

ORD record: ord-c472b62593db49b8b8baa806d5d4e688
Source dataset: uspto-grants-1997_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05665726

Reaction notes

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