HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 22915170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 10910829 | HCID 10910829 | — |
| Catalyst | Isobutyronitrile | HCID 6559 | — |
| Product | HCID 22915170 | HCID 22915170 | 23.7% |
Reaction Steps
Using a procedure analogous to that described in Preparation 8, from 2,6-dimethyl-1,1-dioxo-benzo[d]isothiazole-3-one (2 g), N-bromosuccinimide (1.7 g) and 2,2'-azo-bis(2-methyl-propionitrile (10 mg) was obtained 650 mg of the title compound. m.p. 153°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05665749 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-c633a36c23b44392b4e45bfcef7f4c69 |
| Source note | uspto-grants-1997_09 |