化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dihydro-6,7-dimethoxy-3-nitronaphthalene → trans-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-(4-hydroxymethyl-5-methyl-3-pyridinyl)-2-nitro-naphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dihydro-6,7-dimethoxy-3-nitronaphthalene | HCID 10752220 | — |
| 反応物 | (3-Bromo-5-methyl-4-pyridyl)methyl methoxymethyl ether | HCID 22911326 | — |
| 生成物 | trans-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-(4-hydroxymethyl-5-methyl-3-pyridinyl)-2-nitro-naphthalene | HCID 54195408 | — |
反応手順
The compound of step 14c was condensed with 1,2-dihydro-6,7-dimethoxy-3-nitronaphthalene according to the procedure of Example 13c. The protecting methoxymethyl group was removed from the intermediate by a standard hydrolysis method (HCl, ethanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05668141 |
| 出典データセット | uspto-grants-1997_09 |
| ORD ID | ord-6d128bcaec534abc8e0d097f2016431f |
| 出典メモ | uspto-grants-1997_09 |