HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 1,2,2,6,6-Pentamethyl-piperidin-4-one oxime | HCID 241950 | — |
| Product | N-benzyl-N-(1,2,2,6,6-pentamethylpiperidin-4-yl)hydroxylamine | HCID 22902720 | 40% |
Reaction Steps
Following the procedure of Example 1, the title compound is prepared from 1,2,2,6,6-pentamethylpiperidin-4-one oxime (5.0 g, 27 mmol) and benzyl bromide (4.6 g, 27 mmol) in a 40% yield to give 3.0 g of a white solid which melts at 107°-108° C. after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05668199 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-e176e89fbef64b0090c0bf12dc4cc516 |
| Source note | uspto-grants-1997_09 |