化工社化工社 化学情報印刷レポート · 研究参考用
Sebacic Acid → Bis(tetrabutylammonium)sebacate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sebacic Acid | HCID 5192 | — |
| 反応物 | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Bis(tetrabutylammonium)sebacate | HCID 21903074 | — |
反応手順
The procedure used was the same as described above by titration of sebacic acid (0.814 g, 4.02×10-3 mol) with 1 M tetrabutylammonium hydroxide solution in methanol. After removal of solvent, a quantitative yield (2.75 g) of salt was obtained. FIG. 45 shows a 1H NMR spectrum and FIG. 46 shows a 13C NMR spectrum of the salt in CDCl3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05668224 |
| 出典データセット | uspto-grants-1997_09 |
| ORD ID | ord-52e47b19d50c4cb19f254758061621fb |
| 出典メモ | uspto-grants-1997_09 |