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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1378634생성일: 2026년 10월 25일

Methanol → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanol

https://huagongshe.com/reaction/1378634

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물TetrahydrofuranHCID 8028—
반응물Sodium borohydrideHCID 4311764—
반응물4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehydeHCID 21474525—
용매WaterHCID 962—
생성물4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanolHCID 21474532—

반응 단계

1.6 g (5 mmol) of the aldehyde obtained in Example 45, 50 ml of THF and 50 ml of methanol are introduced into a round-bottomed flask. 100 mg (2.5 mmol) of sodium borohydride are added in small portions and the mixture is stirred at room temperature for 4 h. The reaction medium is poured into water, the mixture is extracted with ethyl ether and the organic phase is separated after settling has taken place, dried over magnesium sulphate and evaporated.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05668156
출처 데이터셋uspto-grants-1997_09
ORD IDord-4f9d7bee45dc4035aeb87ad141ca52c4
출처 메모uspto-grants-1997_09