HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Di-tert-butyl-4-hydroxybenzoyl chloride → Allyl 4-(3,5-di-tert-butyl-4-hydroxybenzoyloxymethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Di-tert-butyl-4-hydroxybenzoyl chloride | HCID 3787187 | — |
| Reactant | Allyl 4-hydroxymethylbenzoate | HCID 22392687 | — |
| Product | Allyl 4-(3,5-di-tert-butyl-4-hydroxybenzoyloxymethyl)benzoate | HCID 21474580 | — |
Reaction Steps
In a manner similar to Example 1(d), by reaction of 7.7 g (28.6 mmol) of 3,5-di-tert-butyl-4-hydroxybenzoyl chloride with 5.5 g (28.6 mmol) of allyl 4-hydroxymethylbenzoate, 4.1 g (34% ) of the expected allyl ester, melting point 100°-1° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05668156 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-ccfbb925e97741929789b163a1fbb9c4 |
| Source note | uspto-grants-1997_09 |