Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dichloroaniline → 2,2'-Dithiobis[N-(3,4-dichlorophenyl)benzamide]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dichloroaniline | HCID 7257 | — |
| 반응물 | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2,2'-Dithiobis[N-(3,4-dichlorophenyl)benzamide] | HCID 18935342 | 10.2% |
반응 단계
This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.04 g, 3.03 mmol) in 25 mL of dichloromethane and 3,4-dichloroaniline (0.982 g, 6.06 mmol) in 8 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes to yield 0.184 g of the title compound, mp 230°-233° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05668291 |
| 출처 데이터셋 | uspto-grants-1997_09 |
| ORD ID | ord-bb12deb70b5c4af48ed5bbe26ac4c221 |
| 출처 메모 | uspto-grants-1997_09 |