HCID 18463313, compound → HCID 11814877, compound

HRID 1379177Notes

Reaction equation

HRID 1379177 reaction equation
[F:1][C:2]1[C:7]([B-:8]([C:31]2[C:36]([F:37])=[C:35]([F:38])[C:34]([F:39])=[C:33]([F:40])[C:32]=2[F:41])([C:20]2[C:25]([F:26])=[C:24]([F:27])[C:23]([F:28])=[C:22]([F:29])[C:21]=2[F:30])[C:9]2[C:14]([F:15])=[C:13]([F:16])[C:12]([F:17])=[C:11]([F:18])[C:10]=2[F:19])=[C:6]([F:42])[C:5]([F:43])=[C:4]([F:44])[C:3]=1[F:45].[H+].[Li].Cl.[CH2:49]([NH+:53]([CH2:58][CH2:59][CH2:60][CH3:61])[CH2:54][CH2:55][CH2:56][CH3:57])[CH2:50][CH2:51][CH3:52]>O>[F:37][C:36]1[C:31]([B-:8]([C:9]2[C:14]([F:15])=[C:13]([F:16])[C:12]([F:17])=[C:11]([F:18])[C:10]=2[F:19])([C:7]2[C:6]([F:42])=[C:5]([F:43])[C:4]([F:44])=[C:3]([F:45])[C:2]=2[F:1])[C:20]2[C:21]([F:30])=[C:22]([F:29])[C:23]([F:28])=[C:24]([F:27])[C:25]=2[F:26])=[C:32]([F:41])[C:33]([F:40])=[C:34]([F:39])[C:35]=1[F:38].[CH2:58]([NH+:53]([CH2:49][CH2:50][CH2:51][CH3:52])[CH2:54][CH2:55][CH2:56][CH3:57])[CH2:59][CH2:60][CH3:61]

Participants

4

Reactant 2

HCID 18463313HCID 18463313, compoundHCID 86750431HCID 86750431, compound

Product 1

HCID 11814877HCID 11814877, compoundYield 80%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Next, 16 mmol of lithium tetrakis(pentafluorophenyl)boric acid was reacted with 16 mmols of tri-n-butylammonium hydrochloride in water to obtain 12.8 mmol of tri-n-butylammonium tetrakis(pentafluorophenyl)borate in the state of a white solid.

Sources & evidence

ORD record
ord-57429d6f2fa348f7a7d27416b0cc9f22
Source dataset
uspto-grants-1997_09
Patent number
US05670580

Reaction notes

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