HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 12548239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Sodium sulfide nonahydrate | HCID 73972 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12548239 | HCID 12548239 | — |
Reaction Steps
A solution of 7.65 g (32 mmol) of sodium sulfide nonahydrate and 8.7 ml (64 mmol) of 2-bromoethylbenzene in 150 ml of 1:1 tetrahydrofuran:methanol was heated at reflux under inert atmosphere. After 24 h, the solution was allowed to cool and concentrated in vacuo to give the crude desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05670675 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-f9d88fd7c2764176b5c20ec852567e45 |
| Source note | uspto-grants-1997_09 |