Borane → 1,5-Diphenylpentan-3-amine

HRID 1379344Notes

Reaction equation

HRID 1379344 reaction equation
[C:1]1([CH2:7][CH2:8][C:9](=[N:18]O)[CH2:10][CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.B>>[NH2:18][CH:9]([CH2:10][CH2:11][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 6331BoraneHCID 225565N-(1,5-diphenylpentan-3-ylidene)hydroxylamine

Product 1

HCID 153888741,5-Diphenylpentan-3-amine

Procedure

According to the procedure of Feuer and Braunstein (J. Org. Chem. 1969, 34, 1817), the resultant compound of Example 31 was treated with borane to give the desired compound.

Sources & evidence

ORD record
ord-cb7c786c8b8c455db8fdadaec64c01f2
Source dataset
uspto-grants-1997_09
Patent number
US05670675

Reaction notes

Loading…