Formaldehyde → HCID 22910140, compound

HRID 1379385Notes

Reaction equation

HRID 1379385 reaction equation
[OH:1][CH:2]([CH:11]([OH:20])[CH2:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[CH2:21]=O.OS(O)(=O)=O>C(O)(=O)C>[C:5]1([CH2:4][CH2:3][CH:2]2[CH:11]([CH2:12][CH2:13][C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)[O:20][CH2:21][O:1]2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 1118Sulfuric AcidHCID 114145663,4-Hexanediol, 1,6-diphenyl-

Product 1

HCID 22910140HCID 22910140, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The resultant compound of Example 149 was treated with paraformaldehyde and H2SO4 in acetic acid according to the procedure of Hough, et. al. (J. Chem. Soc., 1952, 1525) to provide the desired compound.

Sources & evidence

ORD record
ord-45e0bc9a8629432fbeb4af3caa8678ee
Source dataset
uspto-grants-1997_09
Patent number
US05670675

Reaction notes

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