HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → N'-[4(1-chloromethyl-ethenyl)phenyl]-N-methyl urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | N'-[4(1-dimethylaminomethyl-ethenyl)phenyl]-N-methyl urea | HCID 13187360 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N'-[4(1-chloromethyl-ethenyl)phenyl]-N-methyl urea | HCID 13187359 | — |
Reaction Steps
To a solution of 13.85 g (0.06 Mol) N'-[4(1-dimethylaminomethyl-ethenyl)phenyl]-N-methyl urea in 180 ml absolute CH2Cl2 are added dropwise, at 20°-30°, within 20 minutes, 9.4 g (0.06 Mol) chloroformic acid phenyl ester in 50 ml absolute CH2Cl2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579585 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-035c661a6cc34767b205d4d8b37b40a0 |
| Source note | uspto-grants-1986_04 |