Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 7-Methoxybenzofuran | HCID 590462 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 7-Benzofuranol | HCID 78515 | 50% |
Reaction Steps
A mixture of 7methoxybenzofuran (1.8 g.) and pyridine hydrochloride (4.6 g.) was heated at 220° C. for 21/2 hours. The reaction was cooled and diluted with methylene chloride. The solution was washed with 5% aqueous hydrochloric acid (six times); dried (MgSO4) and concentrated to an oil, 0.8 g. (50% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04579865 |
|---|
| Source dataset | uspto-grants-1986_04 |
|---|
| ORD ID | ord-aa093140135c47ccaadabfa77e31dec3 |
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| Source note | uspto-grants-1986_04 |
|---|
