HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 86088-36-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | (Pent-4-en-1-yl)benzene | HCID 517892 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 86088-36-0 | HCID 10855795 | — |
Reaction Steps
5-Phenylpent-1-ene (14.2 g, 0.0973 mol) and m-chloroperbenzoic acid (16.79 g, 0.0973 mol) in dichloromethane (300 ml) was stirred at room temperature for 4 hours. The solution was washed with saturated aqueous sodium hydrogen carbonate solution and dried (MgSO4). The solvent was evaporated off under reduced pressure to give an oil which was distilled to give 2-(3-phenylpropyl)oxirane (b.p. 85° C., 0.4 mm.Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579862 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-205a8488e9cc4405b1ddfb57e7330eaa |
| Source note | uspto-grants-1986_04 |