HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11268015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13335370 | HCID 13335370 | — |
| Product | HCID 11268015 | HCID 11268015 | 69.1% |
Reaction Steps
Sixty grams of thionyl chloride was added to 16.4 g (0.05 mol) of β-(trichlorogermyl)hydrocinnamic acid (7), and the mixture was heated under reflux for 2 hours. Then excess thionyl chloride was distilled away in the usual manner. The residue, upon vacuum distillation, gave 12.9 g of a fraction, bp 148°-149° C./4 mmHg. The yield was 69.1%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579961 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-2b4e152379aa46ec9ead4b63a5b316df |
| Source note | uspto-grants-1986_04 |