HRID1380157

反应详情

EQUATION

反应方程式

HRID 1380157 的结构方程式

PROCEDURE

实验过程

A mixture of 36 g (0.2 mol) of trichlorogermane and 35.2 g (0.2 mol) of ethyl cinnamate was stirred for 2 hours, and then the reaction product was distilled under vacuum to afford 56 g of a fraction, b.p. 169°-170° C./4 mmHg. Yield 78.7%.

WORKUP

后处理

  1. distillationthe reaction product was distilled under vacuum
  2. customto afford 56 g of a fraction, b.p. 169°-170° C./4 mmHg