Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chlorobenzylamine → Cumyluron
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chlorobenzylamine | HCID 66648 | — |
| 반응물 | 1-Methyl-1-phenyl-ethylisocyanate | HCID 2769430 | — |
| 생성물 | Cumyluron | HCID 11709249 | 93.9% |
반응 단계
A mixture consisting of 18.1 g of α,α-dimethylbenzyl-isocyanate and 14.2 g of 2-chlorobenzylamine was allowed to stand for 2 hours at room temperature. The white deposit formed was then filtered off. Washing with n-hexane and recrystallization from ethanol gave 28.5 g of colorless crystal product, m.p. 165°-166° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04579969 |
| 출처 데이터셋 | uspto-grants-1986_04 |
| ORD ID | ord-be49908a3d954b5b89eb40641c730788 |
| 출처 메모 | uspto-grants-1986_04 |