HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 3,3-Dimethyl-1-butene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-Chloro-3,3-dimethylbutane | HCID 76111 | — |
| Product | 3,3-Dimethyl-1-butene | HCID 11210 | — |
| Product | 3,3-Dimethyl-1-butanol | HCID 12233 | — |
| Product | 1,1'-Oxybis(3,3-dimethylbutane) | HCID 22662188 | — |
Reaction Steps
The procedure of Example 1 is followed; instead of using potassium hydroxide, 1 mole of potassium hydroxide and 1 mole of sodium hydroxide is utilized, as well as 2 moles of neohexyl chloride. A conversion of about 50% is attained in this procedure. The yields of neohexene, neohexanol, and dineohexyl ether, based on converted neohexyl chloride, are 70.0 mol-%, 6.1 mol-%, and 7.1 mol-%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579992 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-6fb8936451564dce8d0920781e796168 |
| Source note | uspto-grants-1986_04 |